Optical Heating/Cooling Stages Enable Precise Sample Temperature Control and Real-Time Optical Characterization
The following introduces how GoGo Instruments' optical heating/cooling stages achieve precise temperature control and facilitate real-time optical testing:
1. Precise Temperature Control System
Wide Temperature Range & Accurate Regulation: Utilizing liquid nitrogen cooling combined with resistive heating, these stages enable regulation and control across a broad range from cryogenic to high temperatures. For example, standard configurations support a range of -190°C to 600°C, with temperature stability of±0.1°C and a high resolution of 0.1°C. This high-precision control ensures consistent and reliable experimental conditions.
Flexible Ramp Rates: Users can set heating or cooling rates from 0 to 30°C/min, making them suitable for both fine studies requiring slow gradients and dynamic response observations under rapid temperature changes. Furthermore, multi-segment programmable temperature control allows for pre-setting complex temperature profiles to meet the needs of sophisticated experimental protocols.
Advanced Control Algorithms & Sensor Technology: The built-in PID temperature control module, paired with a PT100 temperature sensor, monitors and feeds back the actual temperature within the chamber in real-time, dynamically adjusting energy input to maintain the target value. This closed-loop design effectively minimizes fluctuations and interference, making it particularly suitable for analyzing temperature-sensitive materials.
2. Real-Time Optical Testing Capabilities
Dual Optical Path Compatibility: Supports both reflective and transmissive optical measurement modes. Users can freely switch based on sample characteristics and research objectives, allowing measurement of surface reflection spectra or transmission absorption properties on the same platform, greatly expanding application boundaries.
Large, High-Throughput Viewport Design: Features a large window made of quartz glass, offering excellent light transmission and corrosion resistance. The window can be manually removed and replaced for specific environmental requirements. Coupled with a gas purge function for frost prevention at sub-zero temperatures, it ensures a clear, fog-free field of view even during low-temperature experiments.
In-Situ Integration with Other Equipment: Models like the CH600S-T can be seamlessly coupled with optical detection tools such as microscopes and Raman spectrometers to form a complete in-situ variable-temperature testing system. Data is synchronized and collected via host computer software, enabling correlation analysis between temperature changes and optical signals, providing powerful support for researching material phase transition mechanisms.
3. Structural Optimizations & Functional Extensions
Gas-Tight Chamber & Vacuum Upgrade Option:The default sealed chamber allows for the introduction of protective gas to prevent oxidation contamination. An optional vacuum system can further reduce pressure to simulate extreme space environments. This is particularly important for advanced experiments requiring an inert atmosphere or ultra-high vacuum conditions.
Compact Sample Stage Design: The small-sized sample stage, crafted for efficient thermal conductivity and heat capacity balance, coupled with a short working distance for objectives (e.g., 5mm), ensures optical path collimation while reducing stray light interference, thereby enhancing signal quality.
Intelligent Software Platform: The accompanying temperature controller features an integrated development kit (IDK), facilitating user-customized programming for automated process control. The graphical interface intuitively displays information such as temperature curves and optical parameter trends, simplifying operational procedures and enhancing data processing efficiency.